Carlos Rexach Itoiz defeated Eduardo Nicolas 7-5 6-2 in the Spain 6 3 qualifying round on clay. The upset overturned the form book — Eduardo Nicolas came in leading the head-to-head 1–0. Carlos Rexach Itoiz claimed a first win over Eduardo Nicolas in two meetings, narrowing the head-to-head to 1–1.
| Date | Tournament | Round | Surface | Winner | Score |
|---|---|---|---|---|---|
| 2001-06-04 | Spain 6 1 | SF | clay | Eduardo Nicolas | 6-4 6-2 |